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High flux rotating anode X-ray diffractometer

A powerful and fast system for single crystal X-ray diffraction analysis

  • High source flux and increased goniometer speed to allow faster experiments
  • Unique telescopic two-theta arm to reach both longer and shorter crystal-to-detector distances
  • Enhanced kappa goniometer design with symmetrical 2θ positioning
  • Improved X-ray optic alignment mechanism for easy maintenance
  • User-inspired cabinet design for improved workflow
  • New electronically controlled brightness of cabinet and crystal lighting
XtaLAB Synergy-R
Protein, Small Molecule
Chemistry, Academic research, Materials science, Geology & minerals, Pharmaceuticals
Single crystal X-ray diffraction, Protein crystallography, Chemical crystallography

XtaLAB synergy-R

The XtaLAB Synergy-R is the most powerful microfocus single crystal X-ray diffractometer available, combining components to allow you to collect high quality diffraction data. Moreover, the XtaLAB Synergy-R offers a number of design features that extend the experimental flexibility to address the most challenging samples. The XtaLAB Synergy-R system is a tightly integrated single crystal X-ray diffractometer with four basic areas of technology: a high-flux, low-maintenance PhotonJet-R X-ray source with continuously variable divergence slit, a high-precision kappa goniometer and Rigaku’s Hybrid Photon Counting (HPC) X-ray detector, the HyPix-6000HE with extremely low noise and high dynamic range, and the CrysAlisPro diffraction software package with sophisticated algorithms to tie the hardware together to minimize the time it takes to measure and solve single crystal X-ray structures.

Benefits:

  • Fast workflow due to complete integration of software and hardware
  • Extremely high performance due to bright source, noise-free detector and fast goniometer speeds
  • Continuously variable divergence lets you resolve reflections from long unit cells.
  • Compact design to fit in your laboratory

Specifications

Product name XtaLAB Synergy-R
Technique Single crystal X-ray diffraction
Benefit 3D structural analysis for molecules and macromolecules
Technology High-flux single crystal X-ray diffractometer
Core attributes X-ray diffractometer with rotating anode X-ray source, kappa goniometer, HPC detector
Core options Oxford Cryostream cooler, XtalCheck-S
Computer External PC, MS Windows® OS, CrysAlisPro Software
Core dimensions 1300 (W) x 1875 (H) x 850 (D) (mm)
Mass 600 kg (core unit)
Power requirements 1Ø, 200-230 V, 20 A 

Accessories

The following accessories are available for this product
ELement ANalyzer

The ELement ANalyzer is a state-of-the-art attachment that allows us to obtain qualitative information on elements in a single crystal at the same time as X-ray diffraction data collection for a single crystal structural analysis. By measuring the X-ray fluorescence spectrum emitted during X-ray diffraction experiments with the ELement ANalyzer, it becomes possible to perform elemental analysis on a single grain of crystal. The ELement ANalyzer can be used for confirmation the presence of central metal(s) in a mononuclear or polynuclear complex or solvent in a crystal for small molecule X-ray crystallography. There is a broad range of possible applications of the ELement ANalyzer in scientific fields.

ELement ANalyzer

ELement ANalyzerは単結晶試料の回折測定と元素分析(定性分析)を並行して行える画期的なアタッチメントです。回折測定中に試料から放出される蛍光X線をELement ANalyzerで計測することにより、結晶に含まれている元素を同定します。Mo線源の装置に組み合わせた場合、P(リン)より重い元素であれば、同定することができます*。RAPIDシリーズやSaturnシリーズなどの単結晶X線回折装置に組み合わせることができ、既存の装置を改造することなく取り付けが可能です。錯体の中心金属の有無や種類、結晶溶媒の有無を数分で確認できるため、無駄となる測定を減らし、研究を効率的に進めることができます。また、多核錯体の確認にも威力を発揮します。

Oxford Cobra

The Oxford Cobra is the non-liquid nitrogen Cryostream. Combining the efficiency of a Cryostream with the advantages of a non-liquid system, the Cobra offers the ultimate solution for both macromolecular and small molecule crystallography.

Oxford Cryostream 800

The 800 Series Cryostream is the most robust, efficient and user-friendly liquid nitrogen based low temperature system available today. Specific features include a superior laminar flow system, meaning virtually zero risk of icing, extremely quiet running and a fast-start system resulting in a cool-down time to 100K of just 20 minutes.

XtalCheck

The XtalCheck system includes software that facilitates both visual and diffraction imaging of crystallization experiments. With the XtalCheck system, one can easily survey many crystallization experiments by eliminating the need to harvest and cryo-cool samples. Moreover, one can perform serial crystallography experiments, by collecting data from multiple crystals, to achieve complete data sets that can be used for structure solution.

XtalCheck

手動タイプ PlateMate

  • シンプルかつ軽量で扱いやすいデザイン
    ゴニオメーターヘッドと同じマウント機構を採用。既存のX線回折装置に簡単に取り付けることができます。SBS規格に準拠した結晶化プレートに対応可能で、MiTeGen社製 In Situ–1 Crystallization Plateでの測定に適したデザインです。
  • 簡単かつ正確なセンタリング機構
    水平および垂直方向に搭載した目盛付きのレールに沿って結晶化プレートを動かすことで、すべてのウェルに対して簡単にセンタリングすることができます。また、微調整機構により、微小な結晶であっても正確なセンタリングが可能です。
  • 結晶化プレート中の結晶を測定
    見分けのつきにくいタンパク質結晶と塩・沈殿剤などの結晶を、ドロップ内から取り出すことなく迅速に判別し、さらに分解能などの品質をチェックできます。
  • 構造解析用のデータ収集も可能
    スクリーニング目的のX線回折像取得のみならず、構造解析用の回折強度データの収集も可能です。結晶化溶媒から取り出すだけで損傷してしまうような特殊な結晶も、その環境下で測定できます。

電動タイプ XtalCheck

  • GUIからコントロール
    すべての機能はGUIから操作できます。
    モーター制御により、微小な結晶であっても正確なセンタリングが可能です。また、複数のウェルや、ドロップ内の複数の結晶を事前に指定することで、簡単な操作で複数の結晶を一度に評価できます。